Single crystal X-ray diffraction facility

About the Single crystal X-ray diffraction facility

The University of Southampton is host to the National Crystallography Service (NCS), which is a unique world leading facility funded by the Engineering and Physical Sciences Research Council (EPSRC) to provide UK academics with access to single crystal X-ray diffraction facilities and expertise beyond those normally available. 

It provides a structure characterisation service and conducts research in chemical crystallography. It is the home to four extremely high powered rotating anode diffractometers, with two copper source and two molybdenum source instruments. These allow us to study a wide range of chemical systems from small molecule organics and pharmaceuticals to anaerobic inorganic complexes and metal organic frameworks (MOFs). These instruments enable study of poorly diffracting or extremely small crystals, down to 10 microns (µ) in each dimension. We also have in-house facilities providing advanced technique studies such as gas cell, high pressure and variable temperature experiments. 

Technical specification

Full details of our instruments can be found on the NCS webpages

"Ada" named in honour of Ada Yonath

  • Rigaku 007HF copper rotating anode
  • HyPix-Arc 100° curved photon counting detector
  • Universal Goniometer (UG2)
  • VHF arc)sec VariMax optics with 70 micrometre (µm) focus
  • Oxford Cryosystems 800 Series CryoStream

"Dot" named in honour of Dorothy Crowfoot Hodgkin

  • Rigaku 007HF copper rotating anode
  • HyPix-Arc 100° curved photon counting detector
  • UG2 with intelligent goniometer head (IGH)
  • VariMax HF optics with 200µm focus
  • Oxford Cryosystems 800 Series CryoStream

"Ros" named in honour of Rosalind Franklin

  • Rigaku FRE+ molybdenum rotating anode
  • HyPix-6000HE hybrid photon counting detector
  • UG2 with IGH
  • VHF arc)sec VariMax optics with 70µm focus
  • Oxford Cryosystems Cobra

"Kat" named in honour of Kathleen Lonsdale

  • Rigaku FRE+ molybdenum rotating anode
  • HyPix-6000HE hybrid photon counting detector
  • UG2 with IGH
  • VariMax HF optics with 100µm focus
  • Oxford Cryosystems Cobra
     

Get in touch

Contact us

School of Chemistry & Chemical Engineering, University of Southampton, University Road, Highfield, SO17 1BJ

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